1-Bromoadamantane CAS 768-90-1

1-Bromoadamantane CAS 768-90-1

CAS NO: 768-90-1
Molecular Formula: C10H15Br
Molecular Weight: 215.13
EINECS NO: 212-200-7
MDL NO: MFCD00074721
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Product Details

Product Description:

Product Name: 1-Bromoadamantane CAS NO:768-90-1


Synonyms:

1-Adamantyl Bromide;

Tricyclo[3.3.1.13,7]decane, 1-bromo-;

 

Chemical & Physical Properties:

Appearance : White to off-white powder.

Assay :≥99.0%

Density:1.448 g/cm3

Boiling Point:240.5℃ at 760 mmHg

Flash Point:96.4℃

Melting Point: 117-120℃

Water Solubility:It is soluble in organic solvents and insoluble in water.

 

 

Uses: It is an intermediate for the synthesis of amantadine hydrochloride.

Production method: derived from the bromination of adamantane. In a dry enamel glass pot, add adamantane, drop bromine, slowly increase the temperature to about 70 ℃, reflux for 6 hours. With the formation of 1-bromoadamantane, the reflux temperature of the reactants gradually increased, and finally reached 100°C. After the reaction, the temperature was left overnight. Then the temperature was raised to 45°C, and sodium bisulfite solution was added dropwise to remove excess bromine. Filter, wash the filter cake with water to neutral, and dry to obtain 1-bromoadamantane.

 

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